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2025, 03, v.44 412-423
不同构型搅拌桨稀土萃取混合槽的性能研究
基金项目(Foundation): 国家自然科学基金资助项目(22078325,22478397)
邮箱(Email): xmh@aaar.com.cn;
DOI: 10.13355/j.cnki.sfyj.2025.03.016
摘要:

萃取混合槽的设计和优化是影响稀土萃取效率的关键因素之一。通过试验与数值模拟对半开式弯叶圆盘式搅拌桨(半开式BWY)、半开式直叶圆盘式搅拌桨(半开式BPY)、闭式弯叶圆盘式搅拌桨(闭式BWY)和闭式直叶圆盘式搅拌桨(闭式BPY)在混合槽中的搅拌性能进行了研究,考察了4种桨型在不同转速下搅拌产生的负压、功率、排量和流场分布。并以闭式BPY为例,对桨叶直径、宽度和弧长,以及圆环内孔直径、混合槽抽吸口直径和桨叶离抽吸口高度6个参数进行了详细的因素分析,建立了搅拌产生的负压、功率准数、湍动能耗散率和排量准数的关联式。研究结果表明:在相同功率条件下,减小桨叶直径和宽度、圆环内孔直径、混合槽抽吸口直径、桨叶离抽吸口高度,增加桨叶弧长,搅拌抽吸能力更强,但桨叶的排量降低。

Abstract:

The design and optimization of extraction mixing tank is one of the key factors affecting the extraction efficiency of rare earth. The mixing performance of semi-open curved-blade disc-type stirring impeller(semi-open BWY),semi-open straight-blade disc-type stirring impeller(semi-open BPY),closed curved-blade disc-type stirring impeller(closed BWY) and closed straight-blade disc-type stirring impeller(closed BPY) paddle in the mixing tank was studied by experiment and numerical simulation. The negative pressure, power, discharge flow rate and flow field distribution generated by the four types of impellers at different rotational speeds were investigated.Taking closed BPY as an example, the six parameters of blade diameter, blade width, blade arc length, inner ring diameter, suction port diameter of the mixing tank, and the height between the blade and the suction port were analyzed in detail.The correlation equations of negative pressure, power number, turbulent kinetic energy dissipation rate and displacement number were established.The results show that under the same power conditions, reducing the blade diameter, inner ring diameter, suction port diameter, height between the blade and the suction port and blade width, as well as increasing the blade arc length, can enhance the mixing suction capacity, but it can reduce the blade displacement.

参考文献

[1] 徐光宪.稀土(上)[M].北京:冶金工业出版社,1995:1-45.

[2] AMARAL J C B S,SOUZA A L,MORAIS C A.Liquid-liquid separation of zirconium and hafnium from nitric liquor in order to obtain nuclear zirconium oxide using TBP as extractant[J].Chemical Engineering Communications,2020,207(1):73-83.

[3] LADE V G,WANKHEDE P C,RATHOD V K.Removal of tributyl phosphate from aqueous stream in a pilot scale combined air-lift mixer-settler unit:process intensification studies[J].Chemical Engineering and Processing,2015,95:72-79.

[4] NERE N K,PATWARDHAN A W,JOSHI J B.Liquid-phase mixing in stirred vessels:turbulent flow regime[J].Industrial & Engineering Chemistry Research,2003,42(17):4146-4146.

[5] 唐谟堂,曹刿.湿法冶金设备[M].长沙:中南大学出版社,2004:187-194.

[6] RAJI M,ABOLGHASEMI H,SAFSARI J,et al.Hydrodynamic study of an emulsion liquid membrane containing carbon nanotube in a mixer-settler:mean size and size distribution of emulsion globules[J].Chemical Engineering Research and Design,2018,139:77-88.

[7] TANG Q,ZHANG J,WU Y X,et al.An experimental study of immiscible liquid-liquid dispersions in a pump-mixer of mixersettler[J].Chinese Journal of Chemical Engineering,2020,28(1):33-45.

[8] 邹洋,王运东,费维扬.混合澄清槽研究进展[J].化工设备与管道,2014,51(5):40-46.ZOU Yang,WANG Yundong,FEI Weiyang.Research progress of mixer-settler extractor[J].Process Equipment & Piping,2014,51(5):40-46.

[9] 黄毅,武斌,陈葵,等.新型大三角桨叶混合槽内流场的数值模拟[J].湿法冶金,2016,35(4):361-364.HUANG Yi,WU Bin,CHEN Kui,et al.Numerical simulation of flow field of a new triangle impeller in mixer-settler[J].Hydrometallurgy of China,2016,35(4):361-364.

[10] 龚姚腾,曾令挥,肖顺根.不同搅拌桨形式对稀土萃取槽内搅拌效果的影响模拟分析[J].湿法冶金,2009,28(1):49-52.GONG Yaoteng,ZENG Linghui,XIAO Shungen.Simulation analysis on stirring effectiveness of different stirring paddle in rare earth extraction tank[J].Hydrometallurgy of China,2009,28(1):49-52.

[11] 侯伟强.混合澄清器搅拌桨的优化设计[J].湿法冶金,2017,36(6):511-514.HOU Weiqiang.Optimization orthogonal design of impeller of mixer-settler[J].Hydrometallurgy of China,2017,36(6):511-514.

[12] 逄启寿,徐金,王海辉,等.搅拌桨结构参数对混合效率的影响[J].中国钨业,2016,31(4):73-77.PANG Qishou,XU Jin,WANG Haihui,et al.Effects of structure parameters of stirring paddle on mixing efficiency[J].China Tungsten Industry,2016,31(4):73-77.

[13] 李少杰,刘继连,景山.泵轮式混合澄清槽泵轮抽吸高度的变化规律试验研究[J].湿法冶金,2019,38(3):254-258.LI Shaojie,LIU Jilian,JING Shan.Variation of pumping height of pump wheel of mixer-settler[J].Hydrometallurgy of China,2019,38(3):254-258.

[14] 阮飞,武茹明,杨文成,等.不同结构稀土萃取槽传输性能对比研究[J].湿法冶金,2019,38(6):501-504.RUAN Fei,WU Ruming,YANG Wencheng,et al.Comparative study of transport performance of rare earth extraction reactor with different structures[J].Hydrometallurgy of China,2019,38(6):501-504.

[15] 倪志南,武斌,陈葵,等.液-液萃取过程中液滴分散特性的数值模拟[J].湿法冶金,2018,37(5):402-406.NI Zhinan,WU Bin,CHEN Kui,et al.Numerical simulation of droplet dispersion in liquid-liquid mixing chamber[J].Hydrometallurgy of China,2018,37(5):402-406.

[16] 冯羽生,严少卿.管式稀土萃取槽中搅拌桨转速优选研究[J].现代矿业,2021,37(4):149-151.FENG Yusheng,YAN Shaoqing.Optimization of impeller speed in tubular rare earth extraction tank[J].Modern Mining,2021,37(4):149-151.

[17] 徐旭升,武斌,陈葵,等.混合澄清槽优化桨叶形式的数值模拟[J].湿法冶金,2020,39(5):434-439.XU Xusheng,WU Bin,CHEN Kui,et al.Numerical simulation of stirring blade with optimized configuration in mixer-settler[J].Hydrometallurgy of China,2020,39(5):434-439.

[18] 谷世良,谭博仁,程全中,等.轴流泵式混合室内水力学特征的数值模拟[J].化工学报,2024,75(3):815-822.GU Shiliang,TAN Boren,CHENG Quanzhong,et al.Numerical simulation of hydraulic characteristics in axial flow pump type mixer[J].CIESC Journal,2024,75(3):815-822.

[19] 逄启寿,徐永谦.稀土萃取混合室进料口压力仿真[J].稀土,2014,35(2):68-71.PANG Qishou,XU Yongqian.Rare earth extraction mixing chamber inlet pressure simulation[J].Chinese Rare Earths,2014,35(2):68-71.

[20] ZOU Y,YE S S,WANG Y D,et al.CFD simulation and PIV measurement of liquid-liquid two-phase flow in pump-mix mixer [J].Journal of the Taiwan Institute of Chemical Engineers,2016,60:15-25.

[21] DEVI T T,KUMAR B.Mass transfer and power characteristics of stirred tank with Rushton and curved blade impeller[J].Engineering Science & Technology,2016,2:730-737

[22] SINGH K K,MAHAJANIS M,SHENOY K T,et al.Computational fluid dynamics modeling of abench-scale pump-mixer:head,power and residence time distribution[J].Industrial & Engineering Chemistry Research,2007,46(7):2180-2190.

[23] ZHAGN Q H,YANG C,MAO Z S,et al.Large eddy simulation of turbulent flow and mixing time in a gas-liquid stirred tank [J].Industrial & Engineering Chemistry Research,2012,51:10124-10131.

[24] BUJALSKI W,JAWORSKI Z,NIENOW A W.CFD study of homogenization with dual Rushton turbines -comparison with experimental results:Ⅱ the multiple reference frame[J].Chemical Engineering Research & Design,2002,80(1):97-104.

[25] FENG X,CHENG J C,LI X Y,et al.Numerical simulation of turbulent flow in a baffled stirred tank with an explicit algebraic stress model[J].Chemical Engineering Science,2012,69:30-44.

基本信息:

DOI:10.13355/j.cnki.sfyj.2025.03.016

中图分类号:TF845

引用信息:

[1]叶志才,谢明辉,向家伟等.不同构型搅拌桨稀土萃取混合槽的性能研究[J].湿法冶金,2025,44(03):412-423.DOI:10.13355/j.cnki.sfyj.2025.03.016.

基金信息:

国家自然科学基金资助项目(22078325,22478397)

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